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• W3154518266 endingPage "118764" @default.
• W3154518266 startingPage "118764" @default.
• W3154518266 abstract "The present study has addressed carbamazepine (CBZ) degradation by hybrid advanced oxidation system of hydrodynamic cavitation (HC) assisted UV/persulfate with composite ZnO/ZnFe2O4 particles. This hybrid system is comprised of several parallel pathways for generation of both OH and SO4∙- radicals. 98.13 ± 1.03% CBZ degradation was obtained at optimum operational conditions: inlet pressure = 9 atm, pH = 4, initial concentration of CBZ = 15 mg/L, UV power = 18 W, Na2S2O8 = 500 mg/L, ZnO/ZnFe2O4 = 500 mg/L. HC alone resulted in 7.70% degradation of CBZ, while the binary HC + Na2S2O8 system resulted in markedly high degradation of 65.73%. Composite ZnO/ZnFe2O4 particles had dual characteristics, viz. photocatalytic activity and a source of Fe2+/Fe3+ ions released through surface leaching. Relative contributions of OH and SO4∙- radicals to CBZ degradation were identified through permutation-combination of different oxidation systems. Thermodynamic and kinetic behaviors of reactions of CBZ with OH and SO4∙- radicals were analyzed using density functional theory (DFT) at B3LYP/6-31 g(d) level. Single electron transfer (SET) between CBZ and SO4∙- was the primary (and thermodynamically favorable) reaction pathway in initiation of degradation. Degradation intermediates revealed ionization of CBZ through SET before hydroxylation and oxidation – which was corroboration of DFT simulations." @default.
• W3154518266 created "2021-04-26" @default.
• W3154518266 creator A5028471245 @default.
• W3154518266 creator A5086348326 @default.
• W3154518266 date "2021-09-01" @default.
• W3154518266 modified "2023-10-18" @default.
• W3154518266 title "Mechanistic analysis of carbamazepine degradation in hybrid advanced oxidation process of hydrodynamic cavitation/UV/persulfate in the presence of ZnO/ZnFe2O4" @default.
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• W3154518266 doi "https://doi.org/10.1016/j.seppur.2021.118764" @default.
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