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- W3156991003 abstract "A comprehensive investigation using x-ray diffractometry has been conducted to study theoptimum mechanical and thermal conditions for the transformation of anatase-to-rutilefrom a titanium dioxide (TiOl) powder. Milling was applied by employing a conventionalball milling instrument and a quasi-high-energy pulveriser and varying the milling period.Heat treatment was performed by calcination at 850, 900, 950, 975, 1000, 1050 and1100°C for 1 hour, being the predicted optimum temperature to obtain fidly rutile powderwas 975°C. Each powder was milled and then calcined prior to the x-ray difiactioninvestigation. X-ray diffraction data were analysed using (1) standard identification andpeak characterisation and (2) Mozulx, an own-developed software to provide strain,crystallite size and size distribution of phases. Results showed that milling speed andmilling up to 24 hours does not significantly change the phases' composition, but enhancesthe transformation temperature. Conventional milling gives better results than pulverising.Conventional milling at 100 rprn for 3 hours reduces the transformation temperature from1100°C to 1000°C. Longer milling, however, does not improve the transformationtemperature. The optimum process is discussed and SEM micrographs are used to supportthe argument" @default.
- W3156991003 created "2021-04-26" @default.
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- W3156991003 date "2005-02-02" @default.
- W3156991003 modified "2023-09-24" @default.
- W3156991003 title "A Comprehensive X-Ray Diffraction Study On Anatase-To-Rutile Transformation Utilising Mechanical And Thermal Approaches" @default.
- W3156991003 hasPublicationYear "2005" @default.
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