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- W3157004124 abstract "Titanium (Ti)-doped UO2 microspheres of three different Ti concentrations (1000, 2000, and 4000 wppm) were synthesized using an internal gelation process. The microspheres were pressed into pellets, and a two-step heat treatment was applied to form monolithic cylindrical pellets with high densities (≥95%TD). Microstructure of these samples consisted of equiaxed grains with >300% increase in average grain size compared to the undoped UO2 pellets. Secondary Ti-rich chemical phases corresponding to a liquid eutectic formed during sintering were observed at grain boundaries of UO2 for samples doped with 4000 wppm Ti. These Ti-rich chemical phases were not observed in 1000 or 2000 wppm Ti samples at microscale using electron microscopy investigations. The 0.02–0.04% lower lattice parameter values for the Ti-doped UO2 samples compared to the undoped UO2 confirms the incorporation of Ti into the UO2 lattice." @default.
- W3157004124 created "2021-04-26" @default.
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- W3157004124 date "2021-08-01" @default.
- W3157004124 modified "2023-09-25" @default.
- W3157004124 title "Microstructural and crystallographic effects of sol-gel synthesized Ti-doped UO2 sintered under reducing conditions" @default.
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- W3157004124 doi "https://doi.org/10.1016/j.jnucmat.2021.153003" @default.
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