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• W3161311938 startingPage "123868" @default.
• W3161311938 abstract "We here discuss the importance of interfacial mixed layer on determination of the middle block Tg (Tg,B) of lamellar-forming hard-b-soft-b-hard ABA triblock copolymers. The detailed morphological characterization is first conducted by scattering measurements and model analyses, which provides the length fraction of B segments (fint,B) existing in the interfacial mixed layer to the overall B block chain. By investigating Tg for the neat triblock copolymers with various middle block lengths and volume fractions of the A blocks (φA), the variation of Tg,B is found to have a correlation with (fint,B). In the later section, the discussion related to Tg,B is made for the samples with cross-linked A block domains prepared via photo reaction. In this design, the original morphology is finely retained after the cross-linking, thereby enabling the extraction of the pure effects of the domain cross-linking on the physical properties. After the domain cross-linking, interestingly, the glass transition temperature of the B middle block (Tg,B) decreases, especially for the sample with φA > 0.5, where the reduction degree of Tg,B is determined by both the segmental density in the interface and fint,B." @default.
• W3161311938 created "2021-05-24" @default.
• W3161311938 creator A5026476015 @default.
• W3161311938 creator A5038493309 @default.
• W3161311938 date "2021-06-01" @default.
• W3161311938 modified "2023-09-23" @default.
• W3161311938 title "Importance of interfacial mixed layer to determine the middle block Tg in lamellar structures of uncross-linked and cross-linked hard-b-soft-b-hard triblock copolymers" @default.
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• W3161311938 doi "https://doi.org/10.1016/j.polymer.2021.123868" @default.
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