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• W3162592058 abstract "An efficient method for the synthesis of deuterated homologation of boronate esters was developed. This discovery uses robust deuterated agent 5-(methyl-d3)-5H-dibenzo[b,d]thiophen-5-ium trifluoromethane sulfonate (DMTT) as d2-methylene source. Mechanistically, base promoted deprotonation of DMTT to generate d2-sulfur-methylene ylide intermediate, which attack the boron atom of boronic ester and followed by 1,2-migration to afford the deuterated boronic homologues. The developed protocol provides a unique approach to achieve one-carbon growth under the practical mild conditions." @default.
• W3162592058 created "2021-05-24" @default.
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• W3162592058 date "2021-08-01" @default.
• W3162592058 modified "2023-10-17" @default.
• W3162592058 title "Green synthesis of α-deuterated boronates using DMTT reagent" @default.
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• W3162592058 doi "https://doi.org/10.1016/j.gresc.2021.05.001" @default.
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