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- W3163544971 abstract "Abstract This work presents the utilization of dual Lewis and BrØnsted solid acid catalysts synthesized from the acidic functionalized abundant wasted palm oil fruit bunch (POFB) derived porous carbon for a one-pot conversion of glucose to 5-HMF under a bi-phasic NMP-H 2 O/MIBK system. The multiscale-porous POFB based carbon with an enhanced surface area ~ 1,600 m 2 .g − 1 was obtained at the optimized preparing condition (1:2 biochar to KOH mass ratio and carbonization at 850 ºC). The impregnated Al 2 O 3 and the sulfonated POFB derived carbon provided the Lewis (PC-Im1AlLA and PC-Im4AlLA) and BrØnsted (PC-Im50BA) acid catalysts possessing total acidity up to 2.4, and 13.0 mmol.g − 1 , respectively. The optimized reaction condition parameters and the synergistic effect of mutually using both acidic catalysts were extensively investigated to achieve the most efficient 5-HMF production performance. The highest 5-HMF yield, glucose conversion, and 5-HMF selectivity of 63.9%, 100%, and 63.9%, respectively, was attained at 120 o C, for 6 hr by employing 0.005:0.04 catalyst mass ratio of PC-Im4AlLA to PC-Im50BA with addition of some NaCl, 1:3 and 3:1 aqueous to organic phase and NMP to H 2 O volume ratios, respectively. Besides, the proposed catalytic system could be recycled for 3 times with less than 20% reduction of 5-HMF production yield." @default.
- W3163544971 created "2021-05-24" @default.
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- W3163544971 date "2021-05-05" @default.
- W3163544971 modified "2023-10-14" @default.
- W3163544971 title "The Implementation of Mutually using Lewis and Brønsted Acidic Functionalized Carbon supported Solid Acid Catalysts derived from Palm Oil Empty Fruit Bunch for 5-Hydroxy Methylfurfural (5-HMF) Production" @default.
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- W3163544971 doi "https://doi.org/10.21203/rs.3.rs-442931/v1" @default.
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