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- W3164698592 abstract "A reaction of N-sulfonyl-1,2,3-triazole with boron trifluoride etherate afforded a (Z)-β-ensulfonylamido fluoride instead of the previously erroneously assigned E isomer. The correction of the stereochemistry was based on a ge-1D ROESY NMR experiment and X-ray crystal structure analyses. Application of the reaction to N-fluoroalkyl-1,2,3-triazoles afforded new (Z)-β-enamido fluorides in a stereoselective manner. A mechanism involving coordination of BF3 with the triazole ring and vinyl diazonium and vinyl cation intermediates was proposed." @default.
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- W3164698592 date "2021-05-25" @default.
- W3164698592 modified "2023-10-17" @default.
- W3164698592 title "Stereoselective Synthesis of (<i>Z</i>)-β-Enamido Fluorides from <i>N</i>-Fluoroalkyl- and <i>N</i>-Sulfonyl-1,2,3-triazoles" @default.
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- W3164698592 doi "https://doi.org/10.1021/acs.orglett.1c01183" @default.
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