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- W3164850668 abstract "Abstract Linarite, PbCuSO 4 (OH) 2 , crystallizes as secondary mineral in form of clusters of crystals in Mine du Pradet at Cap Garonne in France. A tiny single crystal was isolated and its structure was refined from synchrotron diffraction data ( λ = 0.049592 nm): P 12 1 / m 1, a = 467.75(2), b = 563.48(4), c = 967.64(5) pm, β = 102.647(5)°, wR = 0.0544, 819 F 2 values and 56 variables. The proton positions were also refined. The Cu 2+ cations are located within Cu(OH) 2 ribbons and exhibit pronounced Jahn-Teller distortion ( d (Cu–O): 2 × 191.9, 2 × 197.3 and 2 × 252.8 pm). The Cu(OH) 2 ribbons are condensed with the sulfate tetrahedra and the lead cations. The latter are coordinated to eight oxygen atoms in a slightly anisotropic manner. Calculations of the electron localization function (ELF) of PbO (litharge), PbSO 4 (anglesite) and PbCuSO 4 (OH) 2 (linarite) show pronounced lone-pair character for PbO but rather isotropic ELF values around the lead cations in PbSO 4 and PbCuSO 4 (OH) 2 ." @default.
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- W3164850668 date "2021-05-24" @default.
- W3164850668 modified "2023-10-17" @default.
- W3164850668 title "Linarite from Cap Garonne" @default.
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- W3164850668 doi "https://doi.org/10.1515/znb-2021-0041" @default.
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