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- W3174272023 abstract "The authors regret that in the original Full Paper, some characterization and images of the catalyst Cu/MOF-74 from previous reports were incorrectly shown in the main text and in the Supporting Information. The material was therefore resynthesized following the reported procedure and characterized anew. The original Figure 13 should be replaced by Figure 1 below. FT-IR spectra of (a) fresh and (b) reused Cu/MOF-74 catalyst. The characterization of the new materials was carried out by using different instruments, and thus the first paragraph of the Materials and Instrumentation subsection should be updated as follows: All reagents and starting materials were obtained commercially from Sigma-Aldrich and Merck and were used as received without any further purification unless otherwise noted. Nitrogen physisorption measurements were conducted using a Micromeritics 2020 volumetric adsorption analyzer system. Samples were pretreated by heating under vacuum at 150 °C for 3 h. A TGA/DSC 3+, Mettler Toledo was used for thermogravimetric analysis (TGA) with a heating rate of 10 °C/min under a nitrogen atmosphere. X-ray powder diffraction (XRD) patterns were recorded using a Cu Kα radiation source on a D8 Advance Bruker powder diffractometer. Scanning electron microscopy studies were conducted on a S4800-Hitachi Scanning Electron Microscope (SEM). Transmission electron microscopy studies were performed using a JEOL JEM 1010 Transmission Electron Microscope (TEM) at 80 kV. The Cu-MOF-74 sample was dispersed on holey carbon grids for TEM observation. Elemental analysis with atomic absorption spectrophotometry (AAS) was performed on an AA-6800 Shimadzu. Fourier transform infrared (FT-IR) spectra were obtained on an InfraRed Bruker Tensor 37 instrument, with samples being dispersed on potassium bromide pallets. Figures S2–S7 have been updated in a revised Supporting Information file. The authors sincerely apologize for any inconvenience caused and state that this does not change the scientific conclusions of their Full Paper. As a service to our authors and readers, this journal provides supporting information supplied by the authors. Such materials are peer reviewed and may be re-organized for online delivery, but are not copy-edited or typeset. Technical support issues arising from supporting information (other than missing files) should be addressed to the authors. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article." @default.
- W3174272023 created "2021-07-05" @default.
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- W3174272023 date "2021-06-21" @default.
- W3174272023 modified "2023-09-24" @default.
- W3174272023 title "Corrigendum: Synthesis of 1,2‐Dicarbonyl‐3‐enes by Hydroacylation of 1‐Alkynes with Glyoxal Derivatives Using Metal–Organic Framework Cu/MOF‐74 as Heterogeneous Catalyst" @default.
- W3174272023 doi "https://doi.org/10.1002/cplu.202100262" @default.
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