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- W3178100515 abstract "An efficient iodine-mediated method is developed for the synthesis of functionalized 2-(methylthio)-4H-chromen-4-ones by intramolecular cyclization of easily accessible 1-(2-benzyloxy-aryl)-3,3-bis-methylsulfanyl-propenones. The synthesized chromen-4-ones turn out to be a key precursor for various kinds of chemical reactions. Mechanistically, we observed that iodine-mediated intramolecular cyclization of ketene dithioacetal proceeded through a radical pathway. 3-Halo-2-(methylthio)-4H-chromen-4-ones were achieved via various two- or one-pot halogenation approaches." @default.
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- W3178100515 date "2021-07-07" @default.
- W3178100515 modified "2023-10-16" @default.
- W3178100515 title "Iodine-Mediated Synthesis of 2-(Methylthio)-4<i>H</i>-chromen-4-ones and Study of Their Halogenation Reactions" @default.
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- W3178100515 doi "https://doi.org/10.1021/acs.joc.1c00788" @default.
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