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• W3178233872 endingPage "100478" @default.
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• W3178233872 abstract "Solid-state Li batteries require solid electrolytes which have high Li+ conductivity and good chemical/mechanical compatibility with Li metal anodes and high energy cathodes. Structure/function correlations which relate local bonding to macroscopic properties are needed to guide development of new solid electrolyte materials. This study combines diffraction measurements with solid-state nuclear magnetic resonance spectroscopy (ssNMR) and neutron pair distribution function (nPDF) analysis to probe the short-range vs. long-range structure of glass-ceramic Li3PS4-based solid electrolytes. This work demonstrates how different synthesis conditions (e.g., solvent selection and thermal processing) affect the resulting polyanionic network. More specifically, structures with high P coordination numbers (e.g., PS43- and P2S74-) correlate with higher Li+ mobility compared to other polyanions (e.g., (PS3)nn- chains and P2S64-). Overall, this work demonstrates how ssNMR and nPDF can be used to draw key structure/function correlations for solid-state superionic conductors." @default.
• W3178233872 created "2021-07-19" @default.
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• W3178233872 date "2021-11-01" @default.
• W3178233872 modified "2023-10-16" @default.
• W3178233872 title "Investigation of glass-ceramic lithium thiophosphate solid electrolytes using NMR and neutron scattering" @default.
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• W3178233872 doi "https://doi.org/10.1016/j.mtphys.2021.100478" @default.
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