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• W3178437303 abstract "Hafnium is a very valuable metal having many applications which require it to be free from impurities. It does not exist freely in the earth crust and is found to be associated with zirconium ores. The raffinate of Zr purification process is one of the sources for obtaining Hf. Accurate analysis of Hf in presence of Zr is essential for such recovery processes. A Total reflection X-ray Fluorescence (TXRF) method for chemical characterization of Hf containing solution samples, obtained during the various steps of recovery process of hafnium nitrate from the Zr purification process, was developed. The finally obtained solid HfO2 samples were also characterised by TXRF directly without any dissolution. The TXRF results obtained were compared with Inductively Coupled Plasma- Optical Emission Spectrometry (ICP-OES) results for solution samples and were found to be in good agreement. The TXRF method developed has an added advantage that it can analyse the solid samples directly without any dissolution, in addition to requirement of small amount of samples (ng level), economical, fast and no requirement of matrix matched standards." @default.
• W3178437303 created "2021-07-19" @default.
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• W3178437303 date "2021-08-01" @default.
• W3178437303 modified "2023-10-16" @default.
• W3178437303 title "Compositional characterization of hafnium recovered from zirconium purification process using total reflection X-ray fluorescence" @default.
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• W3178437303 doi "https://doi.org/10.1016/j.sab.2021.106235" @default.
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