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• W3178778829 abstract "Three aryl methyl sulfoxides were prepared via the following sequence: synthesis of the menthyl arenesulfenate from the corresponding thiol, diastereoselective oxidation leading to the sulfinate, then reaction with a Grignard reagent. The aryl moiety was substituted with a methyl ester on the ortho position or a nitro group on the ortho or the para position. The sulfenate esters were obtained in fair to excellent yield (42–82%). Four different oxidizing agents were tested to obtain the corresponding sulfinate esters with diastereomeric excesses (de) ranging from 10 to 48%. After separation of the diastereomers and reaction with methyl Grignard reagent, two enantiopure sulfoxides and one enantioenriched sulfoxide (32% ee) were obtained." @default.
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• W3178778829 date "2021-07-02" @default.
• W3178778829 modified "2023-10-17" @default.
• W3178778829 title "Diastereoselective oxidation of menthyl arenesulfenates to sulfinates and access to enantioenriched aryl methyl sulfoxides" @default.
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• W3178778829 doi "https://doi.org/10.1007/s11696-021-01759-9" @default.
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