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- W3179787036 abstract "• Investigated two novel cocrystal hydrates of Arginine-fumaric acid for the Preferential Studies (PE). • Structure-property correlations with respect to the cocrystal structure and their PE in the mother liquor • Efficient enantiomeric resolution of arginine under preferential enrichment condition. Two new hydrate cocrystals, ( RS )-arginine-fumaric acid-H 2 O ( 2 ) and ( S )-arginine-2 fumaric acid-H 2 O ( 3 ), were obtained by the slow evaporation of the saturated aqueous ethanol solution of a 1:1 mixture of S -enriched arginine (33% ee ) and fumaric acid or ( S )-arginine and fumaric acid, respectively. Cocrystals 2 and 3 possess an isostructural molecular organization containing homochiral 1D chains of arginine similar to that of the anhydrous cocrystal of ( RS )-arginine-fumaric acid ( 1 ). The latter showed an efficient “preferential enrichment (PE)”, a unique spontaneous enantiomeric resolution phenomenon by simple recrystallization from the highly supersaturated solution. The formation of unstable cocrystals 2 and 3 seems to have played a crucial role in the enrichment of arginine in the mother liquor under PE crystallization conditions." @default.
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- W3179787036 date "2021-12-01" @default.
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- W3179787036 title "Crystal structure analysis of highly efficient chiral resolution of (RS)-arginine-fumaric acid cocrystal under preferential enrichment conditions" @default.
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- W3179787036 doi "https://doi.org/10.1016/j.molstruc.2021.131073" @default.
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