FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W3183288246> ?p ?o ?g. }

• W3183288246 endingPage "122864" @default.
• W3183288246 startingPage "122864" @default.
• W3183288246 abstract "A single laboratory method performance verification is reported for a rapid sensitive UHPLC-MS/MS method for the quantification of eight cyclic imine and two brevetoxin analogues in two bivalve shellfish matrices: mussel (Mytilus edulis) and Pacific oyster (Crassostrea gigas). Targeted cyclic imine analogues were from the spirolide, gymnodimine and pinnatoxin groups, namely 20-Me-SPX-C, 13-desMe-SPX-C, 13,19-didesMe-SPX-C, GYM-A, 12-Me-GYM, PnTx-E, PnTx-F and PnTx-G. Brevetoxin analogues consisted of the shellfish metabolites BTX-B5 and S-desoxy-BTX-B2. A rapid dispersive extraction was used as well as a fast six-minute UHPLC-MS/MS analysis. Mobile phase prepared using ammonium fluoride and methanol was optimised for both chromatographic separation and MS/MS response to suit all analytes. Method performance verification checks for both matrices were carried out. Matrix influence was acceptable for the majority of analogues with the MS response for all analogues being linear across an appropriate range of concentrations. In terms of limits of detection and quantitation the method was shown to be highly sensitive when compared with other methods. Acceptable recoveries were found with most analogues, with laboratory precision in terms of intra- and inter-batch precision deemed appropriate. The method was applied to environmental shellfish samples with results showing low concentrations of cyclic imines to be present. The method is fast and highly sensitive for the detection and quantification of all targeted analogues, in both mussel and oyster matrices. Consequently, the method has been shown to provide a useful tool for simultaneous monitoring for the presence or future emergence of these two toxin groups in shellfish." @default.
• W3183288246 created "2021-08-02" @default.
• W3183288246 creator A5001693191 @default.
• W3183288246 creator A5015758572 @default.
• W3183288246 creator A5017380913 @default.
• W3183288246 creator A5037726439 @default.
• W3183288246 date "2021-08-01" @default.
• W3183288246 modified "2023-10-01" @default.
• W3183288246 title "Method performance verification for the combined detection and quantitation of the marine neurotoxins cyclic imines and brevetoxin shellfish metabolites in mussels (Mytilus edulis) and oysters (Crassostrea gigas) by UHPLC-MS/MS" @default.
• W3183288246 cites W156008715 @default.
• W3183288246 cites W1767132251 @default.
• W3183288246 cites W1972332551 @default.
• W3183288246 cites W1974511419 @default.
• W3183288246 cites W1976009907 @default.
• W3183288246 cites W1977090434 @default.
• W3183288246 cites W1980583674 @default.
• W3183288246 cites W1988266357 @default.
• W3183288246 cites W1991502159 @default.
• W3183288246 cites W1992927125 @default.
• W3183288246 cites W1994518623 @default.
• W3183288246 cites W1996714203 @default.
• W3183288246 cites W1997169959 @default.
• W3183288246 cites W2002752655 @default.
• W3183288246 cites W2024397272 @default.
• W3183288246 cites W2030337749 @default.
• W3183288246 cites W2030938378 @default.
• W3183288246 cites W2038080280 @default.
• W3183288246 cites W2039184032 @default.
• W3183288246 cites W2042890168 @default.
• W3183288246 cites W2046383054 @default.
• W3183288246 cites W2047584744 @default.
• W3183288246 cites W2049866908 @default.
• W3183288246 cites W2051899866 @default.
• W3183288246 cites W2061188256 @default.
• W3183288246 cites W2067691944 @default.
• W3183288246 cites W2068450737 @default.
• W3183288246 cites W2069855932 @default.
• W3183288246 cites W2069864982 @default.
• W3183288246 cites W2070297436 @default.
• W3183288246 cites W2075710536 @default.
• W3183288246 cites W2084459300 @default.
• W3183288246 cites W2088046495 @default.
• W3183288246 cites W2089762567 @default.
• W3183288246 cites W2103369617 @default.
• W3183288246 cites W2105613642 @default.
• W3183288246 cites W2105649871 @default.
• W3183288246 cites W2106628435 @default.
• W3183288246 cites W2111413033 @default.
• W3183288246 cites W2138188700 @default.
• W3183288246 cites W2142140748 @default.
• W3183288246 cites W2142169231 @default.
• W3183288246 cites W2146858498 @default.
• W3183288246 cites W2158922561 @default.
• W3183288246 cites W2165670868 @default.
• W3183288246 cites W2174561560 @default.
• W3183288246 cites W2192713129 @default.
• W3183288246 cites W2195352021 @default.
• W3183288246 cites W2320119763 @default.
• W3183288246 cites W2326929914 @default.
• W3183288246 cites W2328983208 @default.
• W3183288246 cites W2345480832 @default.
• W3183288246 cites W2345628567 @default.
• W3183288246 cites W2501579585 @default.
• W3183288246 cites W2607720425 @default.
• W3183288246 cites W2752426052 @default.
• W3183288246 cites W2771050955 @default.
• W3183288246 cites W2806005183 @default.
• W3183288246 cites W2809475026 @default.
• W3183288246 cites W2886857307 @default.
• W3183288246 cites W2900869015 @default.
• W3183288246 cites W2903771147 @default.
• W3183288246 cites W2934598752 @default.
• W3183288246 cites W2955231052 @default.
• W3183288246 cites W2955957818 @default.
• W3183288246 cites W2982185377 @default.
• W3183288246 cites W3014128841 @default.
• W3183288246 cites W4235745051 @default.
• W3183288246 cites W4302969804 @default.
• W3183288246 cites W75590408 @default.
• W3183288246 doi "https://doi.org/10.1016/j.jchromb.2021.122864" @default.
• W3183288246 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/34343946" @default.
• W3183288246 hasPublicationYear "2021" @default.
• W3183288246 type Work @default.
• W3183288246 sameAs 3183288246 @default.
• W3183288246 citedByCount "6" @default.
• W3183288246 countsByYear W31832882462021 @default.
• W3183288246 countsByYear W31832882462022 @default.
• W3183288246 countsByYear W31832882462023 @default.
• W3183288246 crossrefType "journal-article" @default.
• W3183288246 hasAuthorship W3183288246A5001693191 @default.
• W3183288246 hasAuthorship W3183288246A5015758572 @default.
• W3183288246 hasAuthorship W3183288246A5017380913 @default.
• W3183288246 hasAuthorship W3183288246A5037726439 @default.
• W3183288246 hasConcept C10390740 @default.
• W3183288246 hasConcept C119128265 @default.
• W3183288246 hasConcept C158278297 @default.
• W3183288246 hasConcept C185592680 @default.
• W3183288246 hasConcept C2776314819 @default.

• next