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- W3183564293 abstract "A series of hydroxylated polystyrene (PS-OH) resins were prepared from macroporous poly(styrene-co-divinylbenzene) by nitration, reductive amination, diazotation and hydrolysis in sequence, and then a series of hyper-cross-linked hydroxylated polystyrene (HCPS-OH) resins were successfully prepared from the PS-OH resins by the Friedel-Crafts post-cross-linking using dichloromethane as an external cross-linker. Benefiting from the synthetic protocol, the HCPS-OH resins showed better adsorption performance for methylene blue in aqueous solution as compared with the corresponding PS-OH resins. HCPS-OH-4, one of the fabricated HCPS-OH resins which had the hydroxyl content of 5.0 mmol g-1 and BET specific surface area of 69.0 m2 g-1, showed the highest adsorption capacity and selectivity for methylene blue. Higher temperature, higher pH, and higher ionic strength were beneficial to adsorption of methylene blue from aqueous solution. HCPS-OH-4 could be regenerated by treatment with 1.0 M HCl methanol solution and deionized water sequentially. Moreover, HCPS-OH-4 retained good adsorption performance for methylene blue even after 5 cycles of adsorption and regeneration, which implied that it was a good candidate for adsorptive removal of methylene blue dye in waste water." @default.
- W3183564293 created "2021-08-02" @default.
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- W3183564293 date "2021-01-01" @default.
- W3183564293 modified "2023-10-16" @default.
- W3183564293 title "Preparation of hyper-cross-linked hydroxylated polystyrene for adsorptive removal of methylene blue" @default.
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- W3183564293 doi "https://doi.org/10.1039/d1ra04265c" @default.
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