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• W3183804526 abstract "The image describes the evolution mechanism of the phases and morphologies during the synthesis process of LNMO with and without veins. Transition metal cation ordering is essential for controlling the electrochemical performance of cubic spinel LiNi 0.5 Mn 1.5 O 4 (LNMO), which is conventionally adjusted by optimizing the high temperature sintering and annealing procedures. In this present work, multiple characterization techniques, including 6,7 Li NMR, XRD and HRTEM, have been combined to trace the phase transformation and morphology evolution during synthesis. It has been illustrated that simultaneous formation of LiMn 2 O 4 (LMO) and LiNiO 2 (LNO) binary oxides and their conversion into highly reactive Li x Ni 3+ y Mn 3.5+ z O ternary intermediate is a thermal dynamically difficult but crucial step in the synthesis of LNMO ternary oxide. A new strategy of modifying the intermediates formation pathway from binary mode to ternary mode using thermal regulating agent has been adopted. LNMO synthesized with thermal regulating agent exhibits supreme rate capability, long-cycling performance (even at elevated temperature) and excellent capacity efficiency. At a high rate of 100 C, the assembled battery delivers a discharge capacity of 99 mAh g −1 . This study provides a way to control the formation pathway of complex oxides using thermal regulating agent." @default.
• W3183804526 created "2021-08-02" @default.
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• W3183804526 date "2022-02-01" @default.
• W3183804526 modified "2023-10-17" @default.
• W3183804526 title "Tuning the phase evolution pathway of LiNi0.5Mn1.5O4 synthesis from binary intermediates to ternary intermediates with thermal regulating agent" @default.
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• W3183804526 doi "https://doi.org/10.1016/j.jechem.2021.05.031" @default.
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