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- W3190405141 abstract "The reductive cyclization of two linear hexasilanes is contrasted, where a methylated precursor yielded a cyclohexasilane while the tert-butyl-functionalized analog unexpectedly yielded a cyclopentasilane. A comprehensive analysis using X-ray diffraction, IR, HR, HRMS, and multinuclear (1H, 13C and 29Si) 1D and 2D NMR spectroscopy identified the 1,2-dihydrodisilane tBuPhHSi-SiHPhtBu as an additional product, which was interpreted as supportive of a mechanism involving silylene elimination. The results of this study may prove informative about substituent effects in the practice of complex organosilicon molecular synthesis." @default.
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- W3190405141 date "2021-09-01" @default.
- W3190405141 modified "2023-10-16" @default.
- W3190405141 title "Isolation of a Cyclopentasilane from Magnesium Reduction of a Linear Hexasilane" @default.
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- W3190405141 doi "https://doi.org/10.1002/ejoc.202100768" @default.
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