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• W3190809246 endingPage "115422" @default.
• W3190809246 startingPage "115422" @default.
• W3190809246 abstract "The synthesis and structural characterization of a series of hitherto unreported sulphido bridged dinuclear Re(III) complexes containing the chelating dithiocarbamato ligands from the reaction between Re 2 (μ-O 2 CCH 3 ) 4 Cl 2 and dithiocarbamates have been reported. The complexes have similar spectral and electrochemical properties which are consistent with the theoretical study. Sodium salts of dimethyldithiocarbamate, diethyldithiocarbamate and pyrrolidinedithiocarbamate react with the quadruply bonded dirhenium(III,III) complex [Re 2 (μ-O 2 CCH 3 ) 4 Cl 2 ] ( 1 ) in ethanol to afford the sulphido bridged dinuclear quadruple-bond cleavage products of the type [Re 2 ( μ -S)(L R ) 4 (OH 2 ) 2 ] ( 2 (L R )) where L R represents the dithiocarbamato ligands [L R = S 2 CNMe 2 , 2 (L Me ); S 2 CNEt 2 , 2 (L Et ) and S 2 CN(CH 2 ) 4 , 2 (L Pyr )]. Complexes 2 (L R ) are the first example of sulphido bridged dinuclear Re(III) complexes containing the chelating dithiocarbamato ligands. The spectral (IR, UV–vis, NMR) and electrochemical properties of this series of complexes are reported. The identity of 2 (L Et ) has been established by single-crystal X-ray structure determination. The electronic structure and the absorption spectra of the complexes are scrutinized by the density functional theory (DFT) and time-dependent DFT (TD-DFT) analyses." @default.
• W3190809246 created "2021-08-16" @default.
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• W3190809246 date "2021-11-01" @default.
• W3190809246 modified "2023-09-27" @default.
• W3190809246 title "Sulphido bridged dinuclear quadruple bond cleavage product from the reaction between Re2(µ-O2CCH3)4Cl2 and dithiocarbamate: An experimental and theoretical study" @default.
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• W3190809246 doi "https://doi.org/10.1016/j.poly.2021.115422" @default.
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