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- W3191805461 abstract "One fascinating and challenging synthetic target in the field of mechanically interlocked molecules is the family of linear [4]catenanes, which are topologically identical to the logo of automobile maker Audi. Herein, we report an all-in-one synthetic strategy for the synthesis of linear metalla[n]catenanes (n = 2-4) by the coordination-driven self-assembly of Cp*Rh-based (Cp* = η5-pentamethylcyclopentadienyl) organometallic rectangle π-donors and tetracationic organic cyclophane π-acceptors. We selected the pyrenyl group as the π-donor unit, leading to homogeneous metalla[2]catenanes and cyclic metalla[3]catenanes via π-stacking interactions. By taking advantage of the strong electrostatic interactions between π-donor units and π-acceptor units, a heterogeneous metalla[2]catenanes and linear metalla[3]catenanes, respectively, could be obtained by the simple stirring of homogeneous metalla[2]catenanes with a suitable tetracationic cyclophane. On this basis, this all-in-one synthetic strategy was further used to realize a quantitative one-step synthesis of a linear metalla[4]catenanes via the self-assembly of cyclic metalla[3]catenanes and tetracationic cyclophanes. All heterogeneous metalla[n]catenanes (n = 2-4) were fully characterized by single-crystal X-ray analysis, NMR spectroscopy and electrospray ionization mass spectrometry." @default.
- W3191805461 created "2021-08-16" @default.
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- W3191805461 date "2021-08-02" @default.
- W3191805461 modified "2023-10-01" @default.
- W3191805461 title "An “All-in-One” Synthetic Strategy for Linear Metalla[4]Catenanes" @default.
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- W3191805461 doi "https://doi.org/10.1021/jacs.1c06689" @default.
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