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- W3192013487 abstract "Abstract BACKGROUND 2,2,3,3‐tetrafluoro‐1‐propanol (TFP) is a good solvent that is applied in the electronic industry. To recover TFP from its aqueous solution, conventional distillation cannot be adopted because TFP and water can form a minimum azeotrope. RESULTS In this work, extractive distillation is applied to separate the azeotropic mixture of TFP and water using 1‐ethyl‐3‐methylimidazolium acetate ([EMIM][Ac]) as an entrainer. Based on the analysis of residual curve map, three processes are designed to separate the mixture. Extractive distillation processes (EDP) I and II consist of an extractive column and two flashes, and EDP III consists of an extractive column, a flash, and a stripper. For evaluating the three processes, total annual cost (TAC), CO 2 emissions and global energy consumption (GEC) are considered into the objective function. CONCLUSION The simulated results show that EDP III with an extractive column, a flash, and a stripper can provide better economic and environmental benefits. Water can be obtained from the extractive column with a molar purity of 99.7%. TFP can be separated from the top of the flash and stripper with a molar purity of 99.7%. Furthermore, the control structure with two‐point temperature for EDP III is explored and it shows good responses for the disturbances of feed flow rate and composition." @default.
- W3192013487 created "2021-08-16" @default.
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- W3192013487 date "2021-08-12" @default.
- W3192013487 modified "2023-09-25" @default.
- W3192013487 title "Process design, evaluation and control for separation of 2,2,3,3‐tetrafluoro‐1‐propanol and water by extractive distillation using ionic liquid 1‐ethyl‐3‐methylimidazolium acetate" @default.
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- W3192013487 doi "https://doi.org/10.1002/jctb.6872" @default.
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