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• W3192014564 abstract "The host-guest chemistry of metal–organic frameworks (MOFs) has been attracting increasing attention owing to the outstanding properties derived from MOFs-guests combinations. However, there are large difficulties involved in the syntheses of the host-guest MOF systems with air-sensitive metal complexes. In addition, the behaviors on host-guest interactions in the above systems at high temperature are not clear. This study reported the synthetic methods for host-guest systems of metal–organic framework and air-sensitive metal complexes via a developed chemical vapor infiltration process. With the synchrotron X-ray powder diffraction (XRPD) measurements and Fourier Transform infrared spectroscopy (FTIR), the successful loadings of Fe(CO) 5 in HKUST-1 and NH 2 -MIL-101(Al) have been confirmed. At high temperatures, the structural and chemical componential changes were investigated in detail by XRPD and FTIR measurements. HKUST-1 was proven to have strong interaction with Fe(CO) 5 and resulted in a heavy loading amount of 63.1 wt%, but too strong an interaction led to deformation of HKUST-1 sub-unit under heating conditions. NH 2 -MIL-101(Al), meanwhile, has a weaker interaction and is chemically inert to Fe(CO) 5 at high temperatures." @default.
• W3192014564 created "2021-08-16" @default.
• W3192014564 creator A5010048767 @default.
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• W3192014564 date "2021-08-03" @default.
• W3192014564 modified "2023-09-25" @default.
• W3192014564 title "Host-Guest Interactions Between Metal–Organic Frameworks and Air-Sensitive Complexes at High Temperature" @default.
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• W3192014564 doi "https://doi.org/10.3389/fchem.2021.706942" @default.
• W3192014564 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/8369409" @default.
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