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• W3196176404 abstract "This paper presents the Outer Plug Standardization – OPS, a novel technique as an alternative for the classic internal standardization using multiple injection in capillary zone electrophoresis is proposed herein. This technique was applied in a new method for the determination of chloride, nitrate and sulfate in rainwater samples. After the injection accuracy was tested and proved to be a minor error source (average 1.26% RSD), the OPS was applied and it improved the intra-day and inter-day precision of the analytical method by 32.5% and 24.7%, respectively. Using a capillary with effective length of 23.5 cm the electrophoretic separation of the three inorganic anions could be achieved in <1 min, with detection limits of 0.05, 0.09 and 0.11 mg L −1 for chloride, nitrate and sulfate, respectively. Also, the statistical t -test was applied to the results obtained for 82 rainwater samples that were collected and analyzed applying both the method developed in this study and the official APHA 4140 method where no statistical difference was noted within a 95% confidence level. • The analyte itself is used in the place of an internal standard. • Precision was improved in 24.6%–32.5% with the new internal calibration strategy. • Cl − , NO 3 − and SO 4 2− were determined in less than 1 min. • The developed method showed good validation results. • Simple BGE with only 2 components." @default.
• W3196176404 created "2021-08-30" @default.
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• W3196176404 date "2021-12-01" @default.
• W3196176404 modified "2023-09-26" @default.
• W3196176404 title "The novel Outer Plug Standardization (OPS) calibration strategy applied in a new method for the high-throughput determination of Cl−, NO3− and SO4−2 in rainwater samples" @default.
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• W3196176404 doi "https://doi.org/10.1016/j.talanta.2021.122820" @default.
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