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- W3196274645 abstract "The electrochemical formation of Sc–Cu alloy was investigated in LiF–CaF2 eutectic molten salt employing various electrochemical methods. Cyclic voltammetry and square wave voltammetry indicate that the reduction of scandium(III) on the tungsten electrode is a one-step reduction process with three electrons transfer. And underpotential deposition of scandium on the copper electrode occurs owing to the depolarization effect, i.e., forming Sc–Cu intermetallic compounds. The thermodynamic properties of the Sc–Cu intermetallic compounds ScCu4, ScCu2, and ScCu in the temperature range of 1153–1223 K were estimated by open-circuit chronopotentiometry. Moreover, the Sc–Cu alloys were prepared by potentiostatic electrolysis and characterized by optical microscope, X-ray diffraction, scanning electron microscopy, and energy dispersive spectroscopy. The results reveal that only Sc–Cu alloy composed of Cu-ScCu4 can be synthesized at low cathodic current density and above eutectic temperature." @default.
- W3196274645 created "2021-08-30" @default.
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- W3196274645 date "2022-10-01" @default.
- W3196274645 modified "2023-10-18" @default.
- W3196274645 title "Cathodic behavior of scandium(III) on reactive copper electrodes in LiF–CaF2 eutectic molten salt" @default.
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- W3196274645 doi "https://doi.org/10.1016/j.jre.2021.08.011" @default.
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