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- W3198391463 abstract "We describe the design, construction, operation, and performance of a simple and versatile semi-batch reactor that is especially useful for measurement of gas/solid reaction rates at pressures in the range of 1 mTorr to 1500 Torr. The reactor operates by repeatedly imposing small AC modulations of reactant gas pressure on top of a much larger DC pressure background. Based on the rate of pressure relaxation following each AC pulse, the reaction rate is determined. Our design is characterized by modular construction from off-the-shelf, ultra-high-vacuum-compatible components, which facilitate easy retrofitting and adaptation to a range of experimental conditions. Automated experiment control and data acquisition is accomplished via a custom National Instruments© LabView virtual instrument. Data analysis is automated using a custom series of Mathworks© Matlab scripts. We demonstrate reactor performance through measurements of hydrogenation kinetics for a composite H2 getter material consisting of 1,4-bis(phenylethynyl)benzene mixed with a palladium/carbon catalyst." @default.
- W3198391463 created "2021-09-13" @default.
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- W3198391463 date "2021-09-01" @default.
- W3198391463 modified "2023-09-23" @default.
- W3198391463 title "Versatile semi-batch apparatus for manometric measurement of gas–solid reaction rates" @default.
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- W3198391463 doi "https://doi.org/10.1063/5.0058181" @default.
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