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- W3198652556 abstract "Abstract In this work, the first examples of inorganic macrocyclic tin‐oxo clusters which are stabilized by sulfate ligands are reported. As determined by X‐ray diffraction and photoelectron spectroscopy analyses, the prepared inorganic Sn 10 ‐oxo cluster displays interesting mixed valence behaviors, with 8 Sn 4+ located at the cyclic skeleton and two Sn 2+ encapsulated in the center. When further introducing Ti 4+ and In 3+ ions to the synthetic systems, heterometallic Sn 2 Ti 6 and SnIn 5 Ti 6 complexes with Ti 6 (SO 4 ) 9 and SnIn 5 (SO 4 ) 12 macrocyclic skeletons were prepared whose configuration and packing models were affected by the ionic radius of incorporated metals. Moreover, comparative CO 2 reduction experiments confirm that such heterometallic composition can significantly improve the catalytic activities of these inorganic macrocyclic oxo clusters. This work represents a milestone in constructing inorganic tin complexes and also macrocyclic metal oxo clusters with tunable configurations and properties." @default.
- W3198652556 created "2021-09-13" @default.
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- W3198652556 date "2021-10-01" @default.
- W3198652556 modified "2023-10-16" @default.
- W3198652556 title "Macrocyclic Inorganic Tin‐Containing Oxo Clusters: Heterometallic Strategy for Configuration and Catalytic Activity Modulation" @default.
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- W3198652556 doi "https://doi.org/10.1002/chem.202103226" @default.
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