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- W3198726095 abstract "Self-assembly of N,N,N',N'-tetrakis(4-carboxyphenyl)-1,4-phenylenediamine with the help of different solvents provides isostructural hydrogen-bonded organic frameworks (HOF-30). Single-crystal X-ray diffraction (SCXRD) analysis reveals HOF-30 possesses 3D ten-fold interpenetrated dia nets connected by two kinds of hydrogen bonds, namely solvent-bridged carboxyl dimers and carboxyl⋅⋅⋅carboxyl dimers. Degassing treatment for HOF-30 yields HOF-30a with 3D ten-fold interpenetrated dia nets but linked with sole carboxyl⋅⋅⋅carboxyl dimers. Reversible hydrogen-bond-to-hydrogen-bond transformation between solvent-bridged carboxyl dimers in HOF-30 and carboxyl⋅⋅⋅carboxyl dimers in HOF-30a has been unveiled by single-crystal and powder X-ray diffraction. In addition, HOF-30a enables the selective adsorption of propyne over propylene according to single-component sorption and breakthrough experiments. The preferred propyne location in HOF has also been identified by SCXRD test." @default.
- W3198726095 created "2021-09-13" @default.
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- W3198726095 date "2021-10-27" @default.
- W3198726095 modified "2023-10-18" @default.
- W3198726095 title "A Solid Transformation into Carboxyl Dimers Based on a Robust Hydrogen‐Bonded Organic Framework for Propyne/Propylene Separation" @default.
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- W3198726095 doi "https://doi.org/10.1002/anie.202110057" @default.
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