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- W3198859943 abstract "• Two new mixed-ligated cobalt phosphonates 1 and 2 incorporating both 5-phosphonatophenyl-1,2,4-tricarboxylic acid and N-donor co-linkers were synthesized successfully. • Both coordination polymers show 3D framework structure composed of cobalt clusters and organic ligands. • Powder X-ray diffraction, thermal stability, IR spectroscopies and magnetic properties have been studied. • The antiferromagnetic interactions are dominated in compound 1 , while the weak ferromagnetic exchange couplings are observed in compound 2 . Two new mixed-ligated cobalt phosphonates, Co 5 (pbtc) 2 (4,4′-bpy) 2 (H 2 O) 4 ·2H 2 O ( 1 ) and Co 4.5 (pbtcH 0.5 ) 2 (bpm)(H 2 O) 6 ·4H 2 O ( 2 ) (pbtcH 5 = 5-phosphonatophenyl-1,2,4-tricarboxylic acid, 4,4′-bpy = 4,4′-bipyridine and bpm = 2,2′-bipyrimidine), are obtained by incorporating 4,4′-bipyridine and 2,2′-bipyrimidine co-ligands, respectively. Compound 1 has infinite chains constructed by the alternative arrangement of Co 3 trimers and Co 2 dimers, which are connected by pbtc 5− and 4,4′-bpy to form a three-dimensional framework structure. For compound 2 , zigzag-like pentamers of Co are connected by pbtc 5− and bpm ligands achieving a different type of three-dimensional framework structure. The lattice water molecules fill in the void space in the framework structures of both compounds. Magnetic measurements show that the antiferromagnetic interactions are dominated in compound 1 , while the weak ferromagnetic exchange couplings are observed in compound 2 ." @default.
- W3198859943 created "2021-09-13" @default.
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- W3198859943 date "2022-01-01" @default.
- W3198859943 modified "2023-10-18" @default.
- W3198859943 title "Two three-dimensional mixed-ligated cobalt phosphonate coordination polymers: Syntheses, crystal structures and magnetic properties" @default.
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- W3198859943 doi "https://doi.org/10.1016/j.molstruc.2021.131456" @default.
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