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• W3198912556 abstract "Formation of Mn x Co3-x O4 yolk-shell microspheres via a solvothermal reaction of hydrated cobalt and manganese nitrates in ethanol is investigated. Spinel nanocrystals of cobalt oxide or cobalt-rich ternary oxide preferentially develop in the system, while manganese-rich hydroxide form Mn(OH)2-type nanosheets. Instead of continuing to grow individually, the nanocrystallites and nanosheets aggregate into large microspheres due to their strong inter-particle interaction. When the proportion of Mn-rich nanosheets is high, therefore the overall density is low, dehydration of hydroxide nanosheets and a surface re-crystallisation lead to formation of a dense and rigid shell, which is separated from a solid or hollow core via a further Ostwald ripening process. The proposed formation mechanism of the yolk-shell structures based on electron microscopic studies would help us to develop yolk-shell structure based multifunctional materials." @default.
• W3198912556 created "2021-09-13" @default.
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• W3198912556 date "2021-01-01" @default.
• W3198912556 modified "2023-09-26" @default.
• W3198912556 title "Formation mechanism of MnxCo3−xO4 yolk–shell structures" @default.
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• W3198912556 doi "https://doi.org/10.1039/d1ra04996h" @default.
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