Matches in SemOpenAlex for { <https://semopenalex.org/work/W3199755455> ?p ?o ?g. }
- W3199755455 endingPage "462548" @default.
- W3199755455 startingPage "462548" @default.
- W3199755455 abstract "• A novel idea to improve the C18 column through forming octadecane into CDs. • Novel octadecylamine-derived carbon dots with applicability in RPLC/HILIC. • Improved hydrophily and separation performance for traditional C18 column. • Retention mechanism explanation by linear solvation energy relationship model. In order to make up for the deficiencies of traditional C18 column for separating strong polar compounds, combined with the good hydrophilicity of carbon dots (CDs), novel octadecylamine-derived CDs denoted as C18-CDs are designed, synthesized and applied in RPLC/HILIC mixed-mode chromatography with good separation performance towards both hydrophobic and hydrophilic compounds. C18-CDs are synthesized by simple one-step solvothermal method using octadecylamine and citric acid as carbon sources, and C18-CDs with proper polarity are collected through column chromatography purification. This C18-CDs decorated silica column showed good separation performance for polycyclic aromatic hydrocarbons and alkylbenzenes under RPLC mode. Hydrophilic compounds including sulfonamides, nucleosides and nucleobases also achieved good resolution in HILIC mode. Hydrophobic and π-π stacking interactions play major retaining roles in RPLC, whereas hydrophilic partitioning and hydrogen bond interactions turn to the main retention interactions under HILIC mode. This C18-CDs/SiO 2 column was applied for the fast detection of chloramphenicol in milk without complex sample pretreatment process. Quantitative relationship between the peak area and the concentration of chloramphenicol was established with linear equation of A = 1677c + 173. Satisfactory spiked recoveries in the range of 94.1–109.0% were obtained. This work not only proposes a simple method for improving the polarity of C18 column through forming octadecane into CDs, but also provides novel CDs with certain hydrophobicity/hydrophily suitable for mixed-mode chromatography." @default.
- W3199755455 created "2021-09-27" @default.
- W3199755455 creator A5000495785 @default.
- W3199755455 creator A5020597164 @default.
- W3199755455 creator A5044366876 @default.
- W3199755455 creator A5050173769 @default.
- W3199755455 creator A5069974428 @default.
- W3199755455 creator A5074358022 @default.
- W3199755455 date "2021-10-01" @default.
- W3199755455 modified "2023-10-18" @default.
- W3199755455 title "Synthesis of octadecylamine-derived carbon dots and application in reversed phase/hydrophilic interaction liquid chromatography" @default.
- W3199755455 cites W1203701383 @default.
- W3199755455 cites W1439574408 @default.
- W3199755455 cites W1906590783 @default.
- W3199755455 cites W1969490208 @default.
- W3199755455 cites W1979299547 @default.
- W3199755455 cites W1994776499 @default.
- W3199755455 cites W1995457198 @default.
- W3199755455 cites W2005020926 @default.
- W3199755455 cites W2013902855 @default.
- W3199755455 cites W2027150727 @default.
- W3199755455 cites W2029253118 @default.
- W3199755455 cites W2052870416 @default.
- W3199755455 cites W2086028855 @default.
- W3199755455 cites W2088856670 @default.
- W3199755455 cites W2233829945 @default.
- W3199755455 cites W2246673500 @default.
- W3199755455 cites W2560565229 @default.
- W3199755455 cites W2586890415 @default.
- W3199755455 cites W2588278653 @default.
- W3199755455 cites W2594423972 @default.
- W3199755455 cites W2608087309 @default.
- W3199755455 cites W2765207026 @default.
- W3199755455 cites W2798115805 @default.
- W3199755455 cites W2806204632 @default.
- W3199755455 cites W2892350756 @default.
- W3199755455 cites W2896158280 @default.
- W3199755455 cites W2921188702 @default.
- W3199755455 cites W2969218450 @default.
- W3199755455 cites W2972035629 @default.
- W3199755455 cites W2984379416 @default.
- W3199755455 cites W2990030469 @default.
- W3199755455 cites W2994413842 @default.
- W3199755455 cites W2997988524 @default.
- W3199755455 cites W3002606832 @default.
- W3199755455 cites W3022522231 @default.
- W3199755455 cites W3028367524 @default.
- W3199755455 cites W3096026444 @default.
- W3199755455 cites W3109185295 @default.
- W3199755455 cites W3129525710 @default.
- W3199755455 cites W3133988819 @default.
- W3199755455 doi "https://doi.org/10.1016/j.chroma.2021.462548" @default.
- W3199755455 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/34537657" @default.
- W3199755455 hasPublicationYear "2021" @default.
- W3199755455 type Work @default.
- W3199755455 sameAs 3199755455 @default.
- W3199755455 citedByCount "10" @default.
- W3199755455 countsByYear W31997554552022 @default.
- W3199755455 countsByYear W31997554552023 @default.
- W3199755455 crossrefType "journal-article" @default.
- W3199755455 hasAuthorship W3199755455A5000495785 @default.
- W3199755455 hasAuthorship W3199755455A5020597164 @default.
- W3199755455 hasAuthorship W3199755455A5044366876 @default.
- W3199755455 hasAuthorship W3199755455A5050173769 @default.
- W3199755455 hasAuthorship W3199755455A5069974428 @default.
- W3199755455 hasAuthorship W3199755455A5074358022 @default.
- W3199755455 hasConcept C116817701 @default.
- W3199755455 hasConcept C166361863 @default.
- W3199755455 hasConcept C178790620 @default.
- W3199755455 hasConcept C179998833 @default.
- W3199755455 hasConcept C185592680 @default.
- W3199755455 hasConcept C2777691172 @default.
- W3199755455 hasConcept C2779348937 @default.
- W3199755455 hasConcept C32909587 @default.
- W3199755455 hasConcept C33347731 @default.
- W3199755455 hasConcept C43617362 @default.
- W3199755455 hasConcept C51724486 @default.
- W3199755455 hasConcept C90260826 @default.
- W3199755455 hasConceptScore W3199755455C116817701 @default.
- W3199755455 hasConceptScore W3199755455C166361863 @default.
- W3199755455 hasConceptScore W3199755455C178790620 @default.
- W3199755455 hasConceptScore W3199755455C179998833 @default.
- W3199755455 hasConceptScore W3199755455C185592680 @default.
- W3199755455 hasConceptScore W3199755455C2777691172 @default.
- W3199755455 hasConceptScore W3199755455C2779348937 @default.
- W3199755455 hasConceptScore W3199755455C32909587 @default.
- W3199755455 hasConceptScore W3199755455C33347731 @default.
- W3199755455 hasConceptScore W3199755455C43617362 @default.
- W3199755455 hasConceptScore W3199755455C51724486 @default.
- W3199755455 hasConceptScore W3199755455C90260826 @default.
- W3199755455 hasLocation W31997554551 @default.
- W3199755455 hasOpenAccess W3199755455 @default.
- W3199755455 hasPrimaryLocation W31997554551 @default.
- W3199755455 hasRelatedWork W1604894604 @default.
- W3199755455 hasRelatedWork W183366027 @default.
- W3199755455 hasRelatedWork W1993794163 @default.
- W3199755455 hasRelatedWork W2013894653 @default.
- W3199755455 hasRelatedWork W2068118433 @default.