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- W3200012816 endingPage "100577" @default.
- W3200012816 startingPage "100577" @default.
- W3200012816 abstract "In recent years, significant advances have been made on photoredox-catalyzed N-radical addition to C-C unsaturated bond via N-H bond cleavage. However, these N-centered radical additions have so far been mostly limited to the alkenes, and to our knowledge, N-radical 5-endo-dig cyclizations of alkynes have been less exploited. Herein, we disclose an 5-endo-dig N-radical cascade cyclization of o-ethynylacetamides by photoredox catalysis involving rare radical cleavage of C-C triple bond, allowing the practical and controllable synthesis of a diverse array of valuable benzoxazinones and 2-hydroxy-3-indolinones in moderate to good yields under mild conditions. Furthermore, a mechanistic rationale for this radical cyclization cascade is supported by various control experiments and theoretical calculations." @default.
- W3200012816 created "2021-09-27" @default.
- W3200012816 creator A5002882639 @default.
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- W3200012816 creator A5017370431 @default.
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- W3200012816 creator A5045982271 @default.
- W3200012816 creator A5056465234 @default.
- W3200012816 creator A5087744964 @default.
- W3200012816 date "2021-10-01" @default.
- W3200012816 modified "2023-10-01" @default.
- W3200012816 title "Controllable synthesis of benzoxazinones and 2-hydroxy-3-indolinones by visible-light-promoted 5-endo-dig N-radical cyclization cascade" @default.
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- W3200012816 doi "https://doi.org/10.1016/j.xcrp.2021.100577" @default.
- W3200012816 hasPublicationYear "2021" @default.
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