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- W3200680596 abstract "In this study, new 1,3,4-thiadiazol derivatives [M1-M5] were prepared by five reactions. The first compound [M1] of the series of 4,3,1-thiadiazole derivatives was prepared by reacting one mole of 2-amino-5-mercapto-4,3,1-thiadiazole with ethyl chloroacetate, then was the reaction of one mole of the compound [M1] with one mole of thiosemicarbazide to prepare the compound [M2]. The compound [M2] was reflux with sodium hydroxide to prepare the compound [M3], and the compound [M4] was prepared from the reaction 2-amino-5-mercapto-4,3,1-thiadiazole with chloroacetic acid. The compound [M4] was reacted with 1,2-phenylenediamine to give the compound [M5]. Physical characteristics, FT-IR, and 1H NMR, 13C NMR spectrum analysis were used to describe the compounds. The antibacterial properties were investigated against Pseudomonas aeruginosa Gram (−)ve and Staphylococcus aureus Gram (+)ve microorganisms." @default.
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- W3200680596 date "2022-01-01" @default.
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- W3200680596 title "Preparation, diagnostics, and biological evaluation of new 1,3,4-thiadiazol derivatives" @default.
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- W3200680596 doi "https://doi.org/10.1016/j.matpr.2021.08.278" @default.
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