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- W3200737194 abstract "Abstract The synthesis of six dimeric spiroketals bearing an estradiol half fused to the 5α- or 5β-epimers of androstane, cholestane, and spirostane nuclei is described. The synthetic procedure comprises the Sonogashira coupling of different steroid alkynes with 2-iodoestradiol 17-monoacetate, followed by Pd-catalyzed spiroketalization. The structural characterization of the obtained hybrid dimers was performed using a combination of 1D and 2D NMR techniques, and was assisted by DFT calculations. Single crystal X-ray diffraction of one of the obtained compounds confirmed the proposed structures." @default.
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- W3200737194 date "2021-09-17" @default.
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- W3200737194 title "Synthesis and Characterization of Hybrid Dimeric Steroid Spiroketals" @default.
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- W3200737194 doi "https://doi.org/10.1055/a-1647-7610" @default.
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