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- W3201479962 abstract "A concise and environmentally friendly protocol was developed for the synthesis of 6-phenylbenzo[h]quinolines. 6-Phenylbenzo[h]quinolines were obtained in good yields via irradiation of (E)-2-phenyl-3-styrylpyridines with a 254 nm UV light (64 W) in EtOH under an argon atmosphere in the presence of TFA. The reaction is a dehydrogenative annulation reaction that proceeds through 6π-electrocyclization, a [1,5]-H shift, 1,3-enamine tautomerization, and elimination of a hydrogen molecule to afford 6-phenylbenzo[h]quinolines. The described protocol not only avoids the usage of a transition metal catalyst and an oxidant but also has the advantages of high atom efficiency and mild reaction conditions." @default.
- W3201479962 created "2021-09-27" @default.
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- W3201479962 date "2021-01-01" @default.
- W3201479962 modified "2023-09-25" @default.
- W3201479962 title "Synthesis of 6-phenylbenzo[<i>h</i>]quinolines <i>via</i> photoinduced dehydrogenative annulation of (<i>E</i>)-2-phenyl-3-styrylpyridines" @default.
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- W3201479962 doi "https://doi.org/10.1039/d1ob01674a" @default.
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