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- W3202022604 abstract "Combining multiple inorganic components is an effective approach to improve the mechanical properties of inorganic–organic hybrid materials. The inorganic components can form interactions with the organic polymer matrix, and there is thus a need to understand the reinforcement mechanism under the optimal combination of organic polymer and inorganic particles. In this work, we prepared a series of dual inorganic particle–based titania/silica–poly(tetrahydrofuran)–poly( ε -caprolactone) (TiO 2 /SiO 2 –PTHF–PCL) hybrids by means of simultaneous cationic ring-opening polymerization and sol–gel reaction. In addition to constructing hybrid networks, the SiO 2 and TiO 2 components play important roles in multiple toughening mechanisms. The prepared dual inorganic hybrids feature enhanced thermal stability and mechanical properties when compared with the ones with a single inorganic component. The optimized mixing of such two inorganic components is identified through mechanical tests, revealing that the hybrid polymer 70 /(Si 0.6 Ti 0.4 ) 30 (70/18/12 mass ratio) has the highest compressive failure strain (80%) and compressive ultimate strength (1.3 MPa) as well as storage modulus (120 kPa), enabling elongation of up to 37% when compared with its original length. We thus find that the dual inorganic component approach is an effective strategy to enhance the mechanical properties of hybrid materials, suggesting potential applications as scaffolds for tissue engineering and soft robotics. • We study the effect of adding SiO 2 and TiO 2 inorganic components to polymer chains on the hybrids' mechanical properties. • Multiple interactions between the two types of oxide components and the polymer chains are formed. • Improved failure strain and stress are achieved by mixing 60% SiO 2 with 40% TiO 2 under the inorganic/organic ratio of 70:30 (wt%)." @default.
- W3202022604 created "2021-10-11" @default.
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- W3202022604 date "2021-12-01" @default.
- W3202022604 modified "2023-10-16" @default.
- W3202022604 title "Flexible inorganic–organic hybrids with dual inorganic components" @default.
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- W3202022604 doi "https://doi.org/10.1016/j.mtchem.2021.100584" @default.
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