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- W3202341705 abstract "In this paper, the MIL-53(Al)-NH2 metal-organic frameworks (MOFs) was prepared based on the anodic electrosynthesis under green conditions. The anodic electrosynthesis as an environmentally friendly procedure was performed in the aqueous solution, room temperature, atmospheric pressure, and in the short reaction time (30 min). Also, the employed procedure was accomplished without the need for the ex-situ salt and base/probase additives as cation source and ligand activating agent at the constant current mode (10.0 mA cm-2). The electrosynthesized MOFs was functionalized with phosphorus acid tags as a novel mesoporous catalyst. This mesoporous catalyst was successfully employed for synthesis of new series (N-methyl-pyrrol)-pyrazolo[3,4-b]pyridines by one-pot condensation reaction of 3-methyl-1-phenyl-1H-pyrazol-5-amine, 3-(1-methyl-1H-pyrrol-2-yl)-3-oxopropanenitrile and various aromatic aldehydes (mono, bis and tripodal). This catalyst proceeded the organic synthetic reaction via a cooperative vinylogous anomeric based oxidation mechanism with a marginal decreasing its catalytic activity after recycling and reusability." @default.
- W3202341705 created "2021-10-11" @default.
- W3202341705 creator A5001909522 @default.
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- W3202341705 creator A5063148617 @default.
- W3202341705 date "2021-09-29" @default.
- W3202341705 modified "2023-09-25" @default.
- W3202341705 title "Anodic electrosynthesis of MIL-53(Al)-N(CH2PO3H2)2 as a mesoporous catalyst for synthesis of novel (N-methyl-pyrrol)-pyrazolo[3,4-b]pyridines via a cooperative vinylogous anomeric based oxidation" @default.
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- W3202341705 doi "https://doi.org/10.1038/s41598-021-97801-7" @default.
- W3202341705 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/8481481" @default.
- W3202341705 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/34588471" @default.