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- W3202388884 abstract "Rh anodic dissolution has been studied in 0.5 M HSO solution in the range from 0.2 V to 1.2 V (RHE) by means of EQCM, cyclic voltammetry, photometry and XPS. Bright pure Rh electroplate ~ 0.5 µm thick on a gold sputtered quartz crystal electrode has been used for electrochemical and microgravimetrical studies.It has been found that increase in Rh electrode mass during anodic process was less than decrease in mass during the cathodic one. The difference established was 120 ± 60 ng cm. The decrease in electrode mass was also determined at = 0.7 ± 0.1V. Linear dependence Δ - has been shown to exist for the anodic process. The presence of Rh(III) compounds in the solution and on the electrode surface has been evidenced by means of photometrical analysis and XPS measurements.The following electrochemical reaction may account for anodic, cathodic and microgravimetric behaviour of Rh electrode in 0.5 M HSO within the range investigated: where (Rh(OH)) is surface layer of Rh(OH) phase. Rh I Rh(OH)3 has been evaluated to be ~ 0.60 V. of Rh electrode is not an equilibrium potential, because Rh(OH) partly dissolves in the electrolyte." @default.
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- W3202388884 date "2001-06-01" @default.
- W3202388884 modified "2023-10-18" @default.
- W3202388884 title "Eqcm Studies of Rhodium Anodic Dissolution in Sulphuric Acid" @default.
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