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• W3203360478 endingPage "8939" @default.
• W3203360478 startingPage "8934" @default.
• W3203360478 abstract "A series of half-sandwich Ir(III) complexes 1-6 bearing an amidato bidentate ligand were conveniently synthesized and applied to the catalytic Leuckart-Wallach reaction to produce racemic α-chiral primary amines. With 0.1 mol% of complex 1, a broad range of ketones, including aryl ketones, dialkyl ketones, cyclic ketones, α-keto acids, α-keto esters and diketones, could be transformed to their corresponding primary amines with moderate to excellent yields (40%-95%). Asymmetric transformation was also attempted with chiral Ir complexes 3-6, and 16% ee of the desired primary amine was obtained. Despite the unsatisfactory enantio-control achieved so far, the current exploration might stimulate more efforts towards the discovery of better chiral catalysts for this challenging but important transformation." @default.
• W3203360478 created "2021-10-11" @default.
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• W3203360478 date "2021-01-01" @default.
• W3203360478 modified "2023-10-18" @default.
• W3203360478 title "Direct reductive amination of ketones with ammonium salt catalysed by Cp*Ir(<scp>iii</scp>) complexes bearing an amidato ligand" @default.
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• W3203360478 doi "https://doi.org/10.1039/d1ob01710a" @default.
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