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- W3203544603 abstract "An organic-inorganic hybrid FeIII–PrIII-included 2-germano-20-tungstate [Pr(H2O)8]2H2[Fe4(H2O)4 (pca)4Ge2W20O72]•34H2O (Hpca = 2-pyridinecarboxylic acid) (1) was hydrothermally prepared. Its polyoxoanion comprises one tetra-FeIII incorporated [Fe4(H2O)4(pca)4Ge2W20O72]8- hybrid entity and two [Pr(H2O)8]3+ ornamental cations. The [Fe4(H2O)4(pca)4Ge2W20O72]8- 2-germano-20-tungstate entity can be regarded as an infrequent S-type [Ge2W20O72]16- cluster pocketed by four [Fe(H2O)(pca)]2+ cations. The S-type [Ge2W20O72]16- cluster could be imagined as condensation of two divacant Keggin [α-GeW10O37]10- segments by sharing two atoms. It is of interest is that carboxyl O and pyridine N atoms on pca ligands concurrently bind with Fe3+ cations in a five-membered heterocyclic fashion to increase the stability of the whole structure. Furthermore, the electrochemical biosensing properties of 1 as the modified electrode material have been investigated for detecting norepinephrine (NPP), showing a low detection limit of 3.25 µmol/L. This work not only enriches structures of heterometallic germanotungstates (GTs), but also expands applications of polyoxometalates (POMs) in the electrochemical biosensing field." @default.
- W3203544603 created "2021-10-11" @default.
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- W3203544603 date "2022-05-01" @default.
- W3203544603 modified "2023-10-18" @default.
- W3203544603 title "A unique organic-inorganic hybrid FeIII–PrIII-included 2-germano-20-tungstate and its electrochemical biosensing properties" @default.
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- W3203544603 doi "https://doi.org/10.1016/j.cclet.2021.09.078" @default.
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