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- W3204202330 abstract "Sb 2 S 3 films were deposited on unheated glass substrates by thermal evaporation and annealed under vacuum atmosphere for 2 hours at different temperatures. Different characterization techniques were used to better understand the behavior of the Sb 2 S 3 material. XRD and Raman spectroscopy confirmed the formation of pure Sb 2 S 3 powder with orthorhombic lattices. The effect of vacuum annealing on the properties of the films was studied. XRD analysis revealed that as-deposited and annealed films at 150 °C were amorphous in nature whereas those annealed at T ≥ 200 °C were polycrystalline. The crystallite size of the films showed a decrease from 75.8 to 62.9 nm with the increase of the annealing temperature from 200 to 250 °C. The Raman showed several peaks corresponding to the stibnite Sb 2 S 3 phase. The surface morphology of the films was examined by AFM. The roughness decreases slightly as the transformation from the amorphous to the crystalline phase occurs. The chemical compositions of Sb 2 S 3 films were analyzed by EDS, revealing that all films were Sb-rich. The optical parameters were estimated from the transmittance and reflectance spectra recorded by UV-Vis spectroscopy. A reduction in the band gap energy from 2.12 to 1.70 eV with the increase of annealing temperature was also found." @default.
- W3204202330 created "2021-10-11" @default.
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- W3204202330 date "2021-10-26" @default.
- W3204202330 modified "2023-09-27" @default.
- W3204202330 title "Effect of vacuum annealing on the properties of one step thermally evaporated Sb<sub>2</sub>S<sub>3</sub> thin films for photovoltaic applications" @default.
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- W3204202330 doi "https://doi.org/10.1051/epjap/2021210101" @default.
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