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- W3204229999 abstract "A three-component sulfonylative spirocyclization of indolyl ynones with aryldiazonium salts and a sulfur dioxide surrogate of DABCO·(SO2)2 has been developed, providing a range of sulfonated spiro[cyclopentenone-1,3'-indoles] in moderate to good yields. This transformation was initiated by an in situ generated arylsulfonyl radical and proceeded efficiently under metal-free conditions, involving a radical-induced dearomative cascade cyclization accompanied by the insertion of sulfur dioxide. This protocol provides an efficient and convenient method to access sulfonated spiroindolenines, and tolerant various functional groups." @default.
- W3204229999 created "2021-10-11" @default.
- W3204229999 creator A5004302460 @default.
- W3204229999 creator A5009884297 @default.
- W3204229999 creator A5029975178 @default.
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- W3204229999 date "2021-09-28" @default.
- W3204229999 modified "2023-10-12" @default.
- W3204229999 title "Metal-Free Sulfonylative Spirocyclization of Indolyl-ynones via Insertion of Sulfur Dioxide: Access to Sulfonated Spiro[cyclopentenone-1,3′-indoles]" @default.
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- W3204229999 doi "https://doi.org/10.1021/acs.orglett.1c02999" @default.
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