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• W3204262541 endingPage "127380" @default.
• W3204262541 startingPage "127380" @default.
• W3204262541 abstract "Developing high-efficient catalysts is crucial for activating peroxymonosulfate (PMS). Fe-N-C catalysts exhibit excellent performance for PMS activation because of the contribution of doped N, Fe-Nx and Fe3C sites. In our work, a series of Fe-N-C catalysts with high-performance was obtained by pyrolyzing Fe-Zn-MOFs precursors. During pyrolysis process, the change of chemical bonds and formation of active sites in the precursor were elucidated by characterization analysis and related catalytic experiments. Graphitic N, Fe-Nx and Fe3C were confirmed to activate PMS synergistically for ciprofloxacin (CIP) degradation. Besides, the catalytic performance was proportional to the amount of doped iron and calcination temperature. Moreover, the Fe-N-C-3-800/PMS system not only displayed good recycling performance, but also had high anti-interference ability. Integrated with quenching and electron paramagnetic resonance (EPR) experiments, a non-radical pathway dominated by 1O2 was proposed. Furthermore, PMS could bond to Fe-N-C-3-800 to form intermediate for charge transfer, thus accelerate electron transfer between CIP and PMS to realize degradation of CIP. Six main pathways of CIP degradation were proposed, which include bond fission of N-C on piperazine ring and direct oxidation of CIP. This study provided a new idea for the design of heterogeneous carbon catalysts in advanced oxidation field." @default.
• W3204262541 created "2021-10-11" @default.
• W3204262541 creator A5002869474 @default.
• W3204262541 creator A5003642180 @default.
• W3204262541 creator A5024778291 @default.
• W3204262541 creator A5047360429 @default.
• W3204262541 creator A5050735958 @default.
• W3204262541 creator A5064340754 @default.
• W3204262541 creator A5076619746 @default.
• W3204262541 date "2022-02-01" @default.
• W3204262541 modified "2023-10-17" @default.
• W3204262541 title "Fe-N-C catalyst with Fe-NX sites anchored nano carboncubes derived from Fe-Zn-MOFs activate peroxymonosulfate for high-effective degradation of ciprofloxacin: Thermal activation and catalytic mechanism" @default.
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