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• W3204472008 abstract "We studied the effect of Mn on the structure and properties of Cd3−xMnxAs2 crystals with x = 0–0.24, synthesized by direct fusion of high-purity elements. Obtained X-ray diffraction patters suggest that the incorporation of Mn promotes a structural phase transition from primary α-Cd3As2 (x = 0) phase to the α''– Cd3As2 (x = 0.24) phase, while at intermediate compositions both phases can coexist. In addition, the increase of Mn content results in the decrease of lattice cell parameters, which effectively saturates for x > 0.13. Microstructural, calorimetric and magnetometry studies suggest that at high Mn content (x = 0.24) secondary MnAs phase appears. Using obtained results, we estimated the solubility limit of Mn in Cd3As2 as x~0.13, which corresponds to the formation of ternary Cd3−xMnxAs2 compound where Cd atoms are partially substituted by Mn. Formation of ternary compound was also suggested by the results for Cd3As2 + MnAs composite systems, where we also observed the presence of CdAs2 phase, which is a byproduct of corresponding reaction. Additional studies suggested that the CdAs2 phase formation in composite system can be prevented if one uses the Cd3−xMnxAs2 compound instead of pure Cd3As2 as a matrix material." @default.
• W3204472008 created "2021-10-11" @default.
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• W3204472008 date "2022-02-01" @default.
• W3204472008 modified "2023-09-26" @default.
• W3204472008 title "Formation of the α''-phase and study of the solubility of Mn in Cd3As2" @default.
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• W3204472008 doi "https://doi.org/10.1016/j.jallcom.2021.162082" @default.
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