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- W3204756154 abstract "Here we present the solid-state thermal Huisgen cycloaddition polymerization of a tripodal triptycene-based AB3-type monomer (1), featuring one azide group at the bridgehead position and three alkyne groups at the 1,8,13-positions. Monomer 1 self-assembles into a “2D + 1D” structure and undergoes polymerization upon heating in the solid state without disrupting the self-assembled structure of the monomer. The resulting polymer is insoluble and likely composed of hyperbranched polymers with cyclic structures, which are highly entangled with one another to form a polycatetane network. The solid-state polymerization of a thin-film of 1 also proceeds successfully while preserving the original surface morphology at the nanoscale. Solid-state thermal Huisgen cycloaddition polymerization of an azide/alkyne-containing tripodal triptycene-based AB3-type monomer assembly, featuring a lamella structure of 2D sheets that consists of nested packing of the triptycene units, proceeds without disrupting the structure and molecular orientation of the monomer assembly, resulting in a covalently networked hyperbranched polymer film." @default.
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- W3204756154 date "2021-12-05" @default.
- W3204756154 modified "2023-10-09" @default.
- W3204756154 title "Structure-preserving Solid-state Thermal Huisgen Cycloaddition Polymerization of a Self-assembled Triptycene-based AB<sub>3</sub>-type Monomer" @default.
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- W3204756154 doi "https://doi.org/10.1246/cl.210476" @default.
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