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• W3205588694 abstract "The 1H DQ Fourier and Laplace-like spectra for a series of cross-linked natural rubber (NR) samples naturally aged during six years are presented and characterized. The DQ build-up curves of these samples present two peaks which cannot be described by classical functions. The DQ Fourier spectra can be obtained after a numeric procedure which introduces a correction time which depends less on the chosen approximation, spin-½ and isolated CH2 and CH3 functional groups. The DQ Fourier spectra are well described by the distributions of the residual dipolar coupling correlated with the distribution of the end-to-end vector of the polymer network, and with the second and fourth van Vleck moments. The deconvolution of DQ Fourier spectra with a sum of four Gaussian variates show that the center and the width of Gaussian functions increase linearly with the increase in the cross-link density. The Laplace-like spectra for the natural aged NR DQ build-up curves are presented. The centers of four Gaussian distributions obtained via both methods are consistent. The differences between the Fourier and Laplace-like spectra consist mainly of the spectral resolution in the favor of Laplace-like spectra. The last one was used to discuss the effect of natural aging for cross-linked NR." @default.
• W3205588694 created "2021-10-25" @default.
• W3205588694 creator A5067677234 @default.
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• W3205588694 date "2021-10-13" @default.
• W3205588694 modified "2023-10-18" @default.
• W3205588694 title "Bimodal 1H Double Quantum Build-Up Curves by Fourier and Laplace-like Transforms on Aged Cross-Linked Natural Rubber" @default.
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• W3205588694 doi "https://doi.org/10.3390/polym13203523" @default.
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