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• W3206274134 abstract "In the present study, four different methods viz. Hydrothermal, Sol-Gel, Solid-state, Co-precipitation methods are used to successfully synthesize the nickel cobaltite (NiCo2O4) nanostructures. The product obtained from the hydrothermal method shows an intermediate behavior between battery-type and pseudocapacitor-type, whereas other methods yield pure battery-type NiCo2O4 nanostructures. Scanning electron microscopy (SEM) examination evaluated the distinct morphology acquired from each methodology, which had a massive effect on the electrochemical performance of the materials as formulated. To assess the electrochemical performance in 2 M KOH electrolyte, techniques such as Galvanostatic charge–discharge (GCD) and cyclic voltammetry (CV) have been used. The greatest specific capacity recorded in the case of sol–gel synthesized product was 617.22C/g at a current density of 1.0 A/g, but significantly enhanced rate-performance is observed in the case of Co-precipitation produced product (568.20C/g at 1.0 A/g and 374.26C/g at 10.0 A/g). The obtained results verified the effect of different methods of synthesis on morphology and electrochemical performance of the same electrode material prepared under identical environmental conditions." @default.
• W3206274134 created "2021-10-25" @default.
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• W3206274134 date "2021-12-01" @default.
• W3206274134 modified "2023-10-03" @default.
• W3206274134 title "Effect of different synthesis methods on morphology and electrochemical behavior of spinel NiCo2O4 nanostructures as electrode material for energy storage application" @default.
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• W3206274134 doi "https://doi.org/10.1016/j.inoche.2021.108996" @default.
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