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• W3206327211 abstract "Sustainable catalysis is the key for the future progress toward biorefinery and bioeconomy. In this work, we designed and developed an inexpensive and eco-friendly [email protected] catalyst for selective hydrogenation of biomass-based platform molecules. A facile synthesized Ni nanoparticles encapsulated in a stabilized carbon support derived from a sacrificial agent copolymer-gel was investigated in the hydrogenation of furfural (FA) to tetrahydrofurfuryl alcohol (THFOL) and levulinic acid (LA) to γ-valeralactone (GVL). The aim is to study the two different reactions over a highly stabilized Ni nanoparticles embedded in the carbon matrix. The [email protected] was found to be active and selective in multi-catalyzed hydrogenation reactions. The Ni nanoparticles with small and ultra-fine sizes are highly dispersed over the carbon matrix. This was concluded through high-resolution micrography images (SEM, TEM) and XRD patterns. In both reactions, a complete conversion of furfural and levulinic acid was achieved with maximum selectivity over the [email protected] catalyst. The effect of reaction temperature, solvent type, reaction time, and H2 pressure were also studied. Overall, optimized reaction conditions were determined, and the [email protected] is easily reusable and exceptionally durable in the studied reaction cycles. The apparent activation energies for FA hydrogenation to THFOL and LA hydrogenation to GVL are 15.4 kJ/mol and 33.6 kJ/mol, respectively." @default.
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• W3206327211 date "2021-12-01" @default.
• W3206327211 modified "2023-09-26" @default.
• W3206327211 title "Immobilized highly dispersed Ni nanoparticles over porous carbon as an efficient catalyst for selective hydrogenation of furfural and levulinic acid" @default.
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• W3206327211 doi "https://doi.org/10.1016/j.jece.2021.106530" @default.
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