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- W3208761362 abstract "New air and moisture stable [PdCl 2 (pySeCH 2 COOH) 2 ] complex devoid of direct Pd–Se bond was synthesized, characterized and utilized as molecular precursor for Pd 17 Se 15 nanoparticles. Experimental evidences indicate that Pd 17 Se 15 occur through the in-situ generation of Pd nanoparticles. • Air and moisture stable [PdCl 2 (pySeCH 2 COOH) 2 ] was synthesised and characterized. • The complex was used as molecular precursor for synthesizing Pd 17 Se 15 nanoparticles. • Though devoid of Pd–Se bond, the complex produces phase pure Pd 17 Se 15 nanoparticles. • Pd 17 Se 15 nanoparticles were formed through in-situ formation of Pd nanoparticles. An air and moisture stable Pd(II) complex with a pyridyl based selenoether ligand was synthesized and characterized with microanalysis, UV–Vis and NMR spectroscopy. The molecular structure of the complex was established by single crystal XRD analysis. The complex upon thermolysis in oleyl amine (OAm) at higher temperatures about 270 °C afforded Pd 17 Se 15 nanoparticles of average dimensions around 14–19 nm. Phase purity, crystal structure and morphology of nanomaterials were assessed by pXRD, EDS and electron microscopy. Growth duration of nanoparticles was found to have profound effect on the particle size of Pd 17 Se 15 nanoparticles. Time dependent studies indicate that the preparation of Pd 17 Se 15 nanoparticles from molecular precursor proceeds via the involvement of Pd nanoparticles." @default.
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- W3208761362 date "2022-01-01" @default.
- W3208761362 modified "2023-09-27" @default.
- W3208761362 title "Preparation and characterization of colloidal Pd17Se15 nanoparticles from a novel Pd(II) pyridyl selenoether molecular precursor" @default.
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- W3208761362 doi "https://doi.org/10.1016/j.ica.2021.120668" @default.
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