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• W3209199368 abstract "Abstract Advanced EPR techniques such as ENDOR and pulsed EPR are used to investigate the enigmatic black coatings of ancient Egyptian mummies, consisting in a complex and heterogeneous mixtures of conifer resins, wax, fat and oil with variable amounts of bitumen. Natural bitumen always contains traces of vanadyl porphyrin complexes that we used here as internal probes to explore the nanoscale environment of V 4+ ions in these black coatings by hyperfine spectroscopy. Four types of vanadyl porphyrins were identified from the analysis of 14 N hyperfine interactions. Three types (referred to as VO-P1, VO-P2 and VO-P3) are present in natural bitumen from the Dead Sea, among which VO-P1 and VO-P2 are also present in black coatings of mummies. The absence of VO-P3 in mummies, which is replaced by another complex VO-P4, may be due to its transformation during preparation of the black matter for embalming. Analysis of 1 H hyperfine interaction shows that bitumen and other natural substances are intimately mixed in these black coatings, with bitumen aggregate sizes not larger than a few nanometres." @default.
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• W3209199368 date "2021-11-01" @default.
• W3209199368 modified "2023-09-25" @default.
• W3209199368 title "Insight into the structure of black coatings of ancient Egyptian mummies by advanced Electron magnetic resonance of vanadyl complexes" @default.
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• W3209199368 doi "https://doi.org/10.21203/rs.3.rs-1023443/v1" @default.
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