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- W3209706054 abstract "The experimental characterization of the electro-peroxone (E-peroxone) process during the elimination of the antibiotic chloramphenicol (CAP) was carried out in a flow plant using a novel flow-through electrolyzer equipped with two anodes and two cathodes in a cascade configuration, anode-cathode-anode-cathode. The H2O2 is formed at the graphite felt cathodes by reducing O2 provided from the oxygen evolution reaction (OER) performed at the Ti|IrO2-Ta2O5 anodes. This electrolyzer avoids employing an air compressor to supply the O2 for the electrosynthesis of H2O2 during the E-peroxone process. The characterization of E-peroxone was performed by using 2 L of a solution containing 0.05 M Na2SO4 at concentrations of CAP from 20 to 50 mg L−1 TOC (48.9–122.3 mg L−1 CAP), studying the influence of pH (3–9), applied current density (5 ≤ j ≤ 15 mA cm−2), and solution flow rate (0.4 ≤ Q ≤ 1.0 L min−1) on the oxidation of CAP. The best performance reached 100% CAP degradation, 63% TOC removal, at pH 3, j = 10 mA cm−2, Q = 0.4 L min−1 and FO3=17.5 mg min−1. The mineralization current efficiency (MCE) and electrolytic energy consumption (EC) were 19% and 0.202 kWh (g TOC)−1, respectively. The comparison of E-peroxone with anodic oxidation aided by H2O2 (AO-H2O2) and ozonation showed the oxidative power sequence E-peroxone > ozonation > AO-H2O2. The evolution of carboxylic acids and inorganic ions was performed by chromatographic and spectrophotometric techniques. Finally, a route of CAP degradation is proposed." @default.
- W3209706054 created "2021-11-08" @default.
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- W3209706054 date "2022-02-01" @default.
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- W3209706054 title "Incineration of the antibiotic chloramphenicol by electro-peroxone using a smart electrolyzer that produces H2O2 through electrolytic O2" @default.
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- W3209706054 doi "https://doi.org/10.1016/j.seppur.2021.120021" @default.
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